Oooh so *that* is what a rotovap is. I am pleased to see that - rotovap aside - my process for removing high boiling solvent from stuff is very similar, albeit much more messy.
@Dr.Mosharraf
4 ай бұрын
😋😋😋
@bananthkumar3708
Жыл бұрын
I am one of your KZitem follower , your videos was really very nice and helpful in my reaserch. Kindly make a video on how to make a crystals of carboethoxycyclopropyltriphenylphosphoniumtetrafluroborate. Sir if you make a video on this topic very helpful my reaserch work.
@Dr.Mosharraf
Жыл бұрын
I will try
@vinitgaikwad7425
Жыл бұрын
Sir, do you recommend any source from where I can get to know all the possible azaeotropic mixtures of solvents
@Dr.Mosharraf
Жыл бұрын
I will make a short video on that
@md.sydulislam4362
Жыл бұрын
Kindly make a video about how to desalt any metal complex or ligand compounds/samples for HRMS characterization.
@ayanchakraborty2631
Жыл бұрын
You can try lyophilization with continuous washing
@md.sydulislam4362
Жыл бұрын
@@ayanchakraborty2631 i tired with my Lyophilized sample. But it did not work. I used NaOH for pH adjustment, and the ligand has some bound hcl too.. Now after metallation reaction, I have lots of Na+ and Cl- that contained in the solid sample..
@ayanchakraborty2631
Жыл бұрын
@md.sydulislam4362, .if your metal complex is soluble in organic solvent, like DCM or Methanol then soluble it in 10% methanol in DCM filter the residue and evaporate the organic solvent to afford your desired metal complex..
@md.sydulislam4362
Жыл бұрын
Thank you. I will try this.
@Dr.Mosharraf
Жыл бұрын
I will try
@ayanchakraborty2631
Жыл бұрын
Kamon acho , dada??
@Dr.Mosharraf
Жыл бұрын
Valo achi. Tumar Kemon cholche?
@ayanchakraborty2631
Жыл бұрын
@@Dr.Mosharraf.. Valo achi..Dada.. Post doc peyechi.. Taiwan a..
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