Sir ...after freeze pump thaw I need to heat my reaction with reflux so if i will remove the cork to adjust reflux tube my reaction system again can fill with gases so what I've to do?
@Dr.Mosharraf
3 ай бұрын
I normally used Schlenk tube or flask and under flow of argon or nitrogen gas I quickly opened and closed. This technique what I have shown here it is completely under argon and refluxed with closed cap.
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